Notations:-
C - Crystal
Co - Collimator
T - Turn Table
Ic - Ionization Chamber
θ - Glancing Angle
Construction:-
Bragg's Spectrometer consists of a collimator containing two slits $S_1$ and $S_2$ made up of lead, through which X-ray is passed.
A turn table is situated in-front of the collimator on which crystal is placed.
Ionization chamber collects the reflected X-ray
Procedure:-
A fine beam of a monochromatic X-ray is made to fall on the crystal.
The crystal reflects the X-rays which are collected by the ionization chamber.
Turn table is rotated till a sharp increase in the intensity is detected.
The sudden increase in intensity suggests that Bragg's Law is satisfied at the given angle θ.
Then the inter-planar spacing can be determined by using Bragg's Law
nλ = 2d.sinθ
The peak in ionization current occurs more than once for different values of "n"
Numerical
Given:-
λ = 0.819 $A^0$ = 0.0819 nm
d = 0.282 nm
To Find:-
Maximum order of Diffraction $(n_{Max})$
Solution:-
The maximum order of diffraction will occur when sin θ = 1
Therefore, from Bragg's Law, we can write that;
$n_{Max} λ = 2d$
$ ∴ n_{Max} = \frac{2d}{λ}$
$ ∴ n_{Max} = \frac{(2 × 0.282)}{0.0819}$
$ ∴ n_{Max} = 6.886$
Hence, we will obtain 6th order maxima and not 7th order maxima
$ ∴ n_{Max} = 6$